Quality control of vegetableoils is becoming more stringent, and strict laws are being enforced, especially for avoiding adulteration. The public bodies that are responsible for the prevention of the adulteration of foodstuffs necessitate methods of analysis that could facilitate large-scale in situ controls. Similarly, oil producers constantly strive to speed up internal qualitycontrol. As a direct consequence, there is an increasing demand for innovative methods of analysis that could guarantee real-time in situ monitoring and provide adequate accuracy. On such bases, the present work addresses the possibility of monitoring qualitative characteristics of vegetableoils through microwavedielectricspectroscopy. To this purpose, the Cole–Cole dielectric parameters of different vegetableoils are evaluated through an innovative automatable procedure that suitably combines traditional TDR measurements, SOL calibration, frequency domain processing, TL modelling and, finally, a minimization routine. The proposed procedure is carried out first on different “pure” oils and, secondly, on some oil mixtures. The obtained results confirm that different dielectric characteristics are associated with different oils, thus confirming the considerable potential of dielectricspectroscopy for quality and anti-adulterationcontrol purposes, especially in view of practical applications.
Quality and anti-adulteration control of vegetable oils through microwave dielectric spectroscopy
CATALDO, Andrea Maria;CANNAZZA, GIUSEPPE;DE BENEDETTO, EGIDIO;TARRICONE, Luciano
2010-01-01
Abstract
Quality control of vegetableoils is becoming more stringent, and strict laws are being enforced, especially for avoiding adulteration. The public bodies that are responsible for the prevention of the adulteration of foodstuffs necessitate methods of analysis that could facilitate large-scale in situ controls. Similarly, oil producers constantly strive to speed up internal qualitycontrol. As a direct consequence, there is an increasing demand for innovative methods of analysis that could guarantee real-time in situ monitoring and provide adequate accuracy. On such bases, the present work addresses the possibility of monitoring qualitative characteristics of vegetableoils through microwavedielectricspectroscopy. To this purpose, the Cole–Cole dielectric parameters of different vegetableoils are evaluated through an innovative automatable procedure that suitably combines traditional TDR measurements, SOL calibration, frequency domain processing, TL modelling and, finally, a minimization routine. The proposed procedure is carried out first on different “pure” oils and, secondly, on some oil mixtures. The obtained results confirm that different dielectric characteristics are associated with different oils, thus confirming the considerable potential of dielectricspectroscopy for quality and anti-adulterationcontrol purposes, especially in view of practical applications.I documenti in IRIS sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.